Nitric Acid, ASTM A, Practice C, (Huey Test) The specimens are boiled for five periods, each of 48 hours, in a 65 per cent solution of nitric acid. The corrosion. employed to measure the relative susceptibility of austenitic stainless steels to intergranular attack. ASTM A Practice C, boiling nitric acid test is also known . Ferric Sulfate – Sulfuric Acid, ASTM A – Practice B (Stretcher Test). Ferric Sulfate Nitric Acid, ASTM A, Practice C, (Huey Test). Nitric Acid, ASTM A

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The test uses a visual inspection of the surface of the bent specimen to determine pass or fail.

Each ASTM A Practice specification includes a list of the grades of stainless steels and the acceptable etch structures for the specific alloys. From macroscopic imaging to Scanning Electron Microscopy, Element provides turnkey metallographic services using state-of-the-art equipment.

The test evaluates the resistance of a226 steels to sensitization and intergranular attack from welding or heat treatment processes. Practice A, the oxalic acid etch test is used as a rapid technique to screen samples of certain stainless steel grades to ensure they are not susceptible to intergranular attack sensitization.

Choosing the correct method s rely on a complete understanding of your material and processes, as well as the concept of corrosion itself. The oxalic acid test is commonly used before the Strauss test to determine if a sample is susceptible; samples that pass method A will generally show low corrosion rates in the Strauss test.

G2MT Labs is one of the few labs to offer all five ASTM A corrosion testing practices, as well as the expertise to help you atsm which tests to use, what to do if a test fails, and other corrosion consulting as needed.

Corrosion Testing

The Oxalic Acid test is only used to ensure that no corrosion exists; samples are labeled either “Acceptable” or “Suspect”. The samples are weighed at each interval to determine mass loss and degree of susceptibility to intergranular attack. What is your typical turnaround time?

If materials with incorrect heat treatment enter service, they are liable to crack or fail by intergranular corrosion IGC much more rapidly than properly qstm materials; ASTM A is a screening test to help find batches that are incorrectly processed.

Practice E, the Strauss test, is performed to assess attack associated with chromium-rich carbide formation; it does not detect susceptibility to sigma phase formation.


Intergranular Corrosion Testing: An Overview of ASTM A262

Discover perspectives, resources, and advice from our world-leading Engaged Experts. We provide intergranular corrosion evaluation, salt spray testing, stress corrosion, and various other methods to simulate exposure of your products or materials to corrosive environments.

Share on Tumblr Print. The etch structure types used to classify the specimens are: A bend test followed by a visual or micro-examination are used to determine “Pass” or “Fail” of test specimens.

Learn more about our laboratories – where they are located; the unique capabilities they have and how they can help you solve your technical and commercial challenges.

ASTM A is a common intergranular corrosion testing method that can quickly screen batches of material to determine corrosion susceptibility. Some specific hazards statements are given in Contact us now for pricing or a quote! Sensitization causes the grain boundaries of a material to precipitate, creating carbide deposits and causing the material to be susceptible to intergranular attack. This test is used exclusively to determine corrosion in areas high in chromium carbide formations, and is not as effective for intergranular attack caused by other means.

Metals like stainless steels and aluminum contain elements such as niobium and chromium, often integrated because of their natural corrosion resistance.

ASTM A Intergranular Corrosion Testing and Analysis

Choosing an Intergranular Corrosion Test Method Since high temperature processing such as heat treatment is a common practice, many manufacturers wish to perform intergranular corrosion qualification testing on each batch, to ensure that the material has been practie correctly and does not show signs of corrosion susceptibility.

Link to Active This link will always route to the current Active version of the standard. This practice includes boiling the sample for 24 to hours in the solution above, and measures the materials performance quantitatively.

Practice F, is a hour weight-loss based analysis that provides a quantitative measure of the materials performance, and is commonly used to analyze as-received stainless steels.

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At the conclusion off the test, specimens are either visually examined or measured for weight loss and compared to an established corrosion rate for that specific material type. How do you select the right ASTM corrosion practuce method for your material?

The test is generally performed for acceptance of materials, but not sufficient for rejection of materials. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. This website uses cookies to improve user experience. See Appendix X1 for information regarding test selection. Like what you saw? To understand intergranular corrosion testing or intergranular attack commonly abbreviated as IGC or IGAit is important to understand what causes the process to occur.


Based on your materials, application, and requirements, the other 4 methods provide specific focuses. By using our website you consent to all cookies in accordance with our Cookie Policy.

Please refer to the specification for more details. The inch-pound equivalents are in parentheses and may be approximate.

Because it can be run quickly for screening, we often run this test first. This method is a hour boiling test for “as received” specimens of stainless steel.

If you are not sure, please contact us for assistance. The Strauss test is commonly used to evaluate the heat-treatment of as-received material, the effectiveness of alloying additions of elements such as Nb and Ti, or the effectiveness of reducing carbon content to resist intergranular attack. Methods for preparing the test specimens, rapid screening tests, apparatus setup and testing procedures, and calculations and report contents are described for each testing practice.

The Oxalic Acid test is also only applicable to corrosion associated with chromium carbide precipitates and is only useful for specific material grades. This specification covers the standard practices for detecting susceptibility to intergranular attack in austenitic stainless steels. In many cases we can reduce that to as little as 24 hours more than the required testing time if you need fast results.

This simple etching technique is used as a quick screening method to ensure that a sstm is free of intergranular corrosion susceptibility. The ASTM A tests can determine if the proper heat treatment was performed or if the alloys are in danger of intergranular corrosion occurring in use. The first and fastest step is the ASTM A Practice A, a rapid same-day screening method in Prractice acid to determine the susceptibility to intergranular corrosion.

Intergranular corrosion shows up as the dark black lines around the grain boundaries. Please specify the maximum allowable corrosion rate and any available data on the sensitizing heat treatment performed.

Work Item s – proposed revisions of this standard.

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